Multi-anvil Press at Caltech 

This is one of our main research tools, the 1000-ton multi-anvil press in Professor Paul Asimow's lab:

press
 
Curious George for scale

The press uses two separate modules which switch in and out on a convenient rail system: a 6-8 type Walker module and a Getting-designed cubic-anvil module.

Walker Module

The Walker module is used for achieving pressures up to 25 GPa. In this device, six anvil "wedges" press on 8 cubes which in turn press on an octahedral press medium. This is a schematic cross-section of the module:

module2.gif
(picture shamelessly copied from the Rockland Research website)

This stuff goes inside the module:

MAschematic.jpg

We have calibrated the press using a variety of sample assemblies, using both castable ceramic and semi-sintered ceramic pressure media. One of our workhorse configurations is the 14/8 assembly:
This graph shows the pressure calibration for the 14/8 (ram force vs. the pressure of "fixed" transitions):

calgraph.jpg
 
open squares: reversal obtaining low-pressure phase
closed squares: reversal obtaining high-pressure phase
diamonds: electrical resistivity change accompanying Bi transition

Cubic-anvil Module

In the cubic-anvil module, six anvils press on a cubic pressure medium. This device, as currently configured, can attain pressures up to 6 GPa on samples comparable in size to those used in a 0.5" piston-cylinder cell.

More information coming soon

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