The press uses two separate modules which switch in and
out on a convenient rail system: a 6-8 type Walker module and a Getting-designed
cubic-anvil module.
Walker Module
The Walker module is used for achieving pressures up to 25 GPa. In this
device, six anvil "wedges" press on 8 cubes which in turn press on an octahedral
press medium. This is a schematic cross-section of the module:
(picture shamelessly copied from the
Rockland Research
website)
This stuff goes inside the module:
We have calibrated the press using a variety of sample assemblies, using
both castable ceramic and semi-sintered ceramic pressure media. One of our
workhorse configurations is the 14/8 assembly:
- 14 mm edge length octahedron made of semi-sintered MgO plus 5 wt%
Cr2O3
- Toshiba grade-F WC cubes with a truncated edge length of 8 mm
- Stepped LaCrO3 heater
- Pyrophyllite gaskets with a cross section of 2.8 x 4.5 mm
This graph shows the pressure calibration for the 14/8 (ram force vs.
the pressure of "fixed" transitions):