| Facilities
for Mineral Synthesis |
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| e have laboratory facilities that obtain an enormous
range of pressure and temperature conditions, enabling
synthesis of natural and artificial materials under conditions
resembling any that occur in the upper 700 km of the Earth
or in space. The pictures below show the kinds of apparatus
we use for high temperature work at ambient, crustal, upper
mantle, and transition zone pressures, respectively. |
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Piston-Cylinder
apparatus for mineral synthesis. This instrument routinely
operates at 1300°C and at 30 kbar pressure. |
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Components which confine the sample while at high pressure.
The actual sample is the tiny speck to the left of the white
vial near the front with the cork top. |
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The internal assembly which constitute the sample cell.
The sample, itself, is contained in the small Pt capsule at
the left. |
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1700°C controlled-atmosphere furnaces for mineral synthesis.
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Our
1000-ton hydraulic press for
multianvil high-pressure modules waiting, under a typical Caltech
archway, to be hoisted into the lab three floors above. |
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A birds-eye view of the
cubic multianvil device partially assembled. This apparatus
reaches pressure between 3 and 6 GPa with a sample volume
of ~100 cubic millimeters. |
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This photo shows the tungsten
carbide anvils of the octahedal multiannvil device all prepared
for a high pressure run (with pyrophyllite gaskets, cardboard
backing, and teflon tape; the gaskets will be turned towards the
center when the assembly is built). With 8 mm edge length
triangular truncations, this assembly reaches pressure of at
least 14 GPa with a sample volume of ~3 cubic millilmeters. |
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A reflected-light photomicrograph of an
experimental synthesis product. The fibrous grey-brown
materials is a mica, phlogopite. The large blades and six-pointed
stars are plagioclase. We're not really sure why this run
crystallized in such a striking pattern. |
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